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1 article(s) from Fik, Christoph P

Highly reactive, liquid diacrylamides via synergistic combination of spatially arranged curing moieties

Maximilian Maier,
Magnus S. Schmidt,
Markus Ringwald and
Christoph P. Fik

Beilstein J. Org. Chem. 2017, 13, 372–383, doi:10.3762/bjoc.13.40

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Graphical Abstract

Scheme 1: Top: Overview of the synthesized crosslinkers 1–6 and their correlation to each other via formal re...

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Scheme 2: Synthetic pathways to structurally related compounds 1–6.

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Scheme 3: Byproducts 8a and 9a.

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Scheme 4: Synthetic pathways towards the planned cis-intermediate 19.

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Scheme 5: Comparison of structural elements of 1–6 in the ¹H NMR spectra (400 MHz).

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Figure 1: Refractive indices (RI) and viscosities (η) of crosslinkers 1–6 (* solid at room temperature).

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Figure 2: Exemplary photo-DSC plots for the curing of 1 and 3–6 at 37 °C.

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Figure 3: t_max for the curing of 1 and 3–6 at 37 °C (* no polymerization heat detected).

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Figure 4: R_{p, max} for the curing of 1–6 at 37 °C for a) top: ∆H_p of allyl groups = 87.5 kJ·mol⁻¹ and b) botto...

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Figure 5: Polymerization heat, ∆H_p for the curing of 1–6 at 37 °C (* no polymerization heat detected).

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Figure 6: FTIR spectra of 1–6 before (top) and after (bottom) curing; the arrows indicate emerging, character...

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Scheme 6: Proposed reaction pathways for the intramolecular propagation within 1.

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Figure 7: Flexural strength (FS) and E-modulus of cured crosslinkers 1–6; letters refer to statistical groups...

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Full Research Paper

Published 27 Feb 2017

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